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Standard Addition Method
The determination in Problem 15-9 was modified to use the standard-addition method. In this case, a 3.925-g tablet was dissolved in sufficient 0.10 M HCl to give 1.000 L. Dilution of a 20.00-mL aliquot to 100 mL yielded a solution that gave a reading of 415 at 347.5 nm. A second 20.00 -mL aliquot was mixed with 10.0 mL of 50-ppm quinine solution before dilution to 100 mL. The fluorescence intensity of this solution was 503 . Calculate the percentage of quinine in the tablet. | Numerade
The determination in Problem 15-9 was modified to use the standard-addition method. In this case, a 3.925-g tablet was dissolved in sufficient 0.10 M HCl to give 1.000 L. Dilution of a 20.00-mL aliquot to 100 mL yielded a solution that gave a reading of 415 at 347.5 nm. A second 20.00 -mL aliquot was mixed with 10.0 mL of 50-ppm quinine solution before dilution to 100 mL. The fluorescence intensity of this solution was 503 . Calculate the percentage of quinine in the tablet. | Numerade
numerade.com
Aug 7, 2020
Method of Standard Addition
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